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Methods General experimental procedure for the synthesis of α-functionalized propargylamines An oven-dried Schlenk tube of 25 mL equipped with a magnetic stir bar was charged with formamide ( a , 0.4 mmol), terminal alkyne ( b , 0.2 mmol), and anhydrous 1,4-dioxane (1.0 mL), followed by the addition of Grignard reagent ( c , 0.6 mmol)